Solid-phase catch,activate, and release synthesis of cyanine dyes |
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Authors: | Mason Stephen J Balasubramanian Shankar |
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Institution: | University Chemical Laboratory, University of Cambridge, Lensfield Road, Cambridge CB2 1EW, UK. |
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Abstract: | reaction: see text] Trimethine cyanine dye was synthesized by capture and activation of a hemicyanine intermediate on sulfonyl chloride resin followed by reaction and concomitant cleavage by a heterocyclic carbon nucleophile. A small array of dyes were synthesized and characterized to demonstrate the versatility of this chemistry for a number of hemicyanines and heterocyclic nucleophiles. |
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