Structure Elucidation and NMR Characterization of Two New Cyclophane Derivatives |
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| Authors: | Egyed Orsolya Taticchi Aldo Minuti Lucio Gács-Baitz Eszter |
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| Institution: | (1) Institute of Chemistry, Chemical Research Center of the Hungarian Academy of Sciences, H-1525 Budapest, P. O. Box 17, Hungary;(2) Dipartimento di Chimica, Universita degli Studi di Perugia, Via Elce di Sotto 8, 06123 Perugia, Italy |
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| Abstract: | In the course of our on-going investigation to develop synthetic methods for helical cyclophanes using Diels–Alder methodology, a great variety of polycyclic aromatic compounds have been formed. In some cases, the cycloaddition reactions, in addition to the target compounds, gave rise to unexpected products, which were identified by spectroscopic methods. The structure determination based on NMR measurements and semiempirical calculations of two such new compounds are presented in this paper. |
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| Keywords: | Cyclophanes 1H and 13C NMR spectroscopy molecular structures semiempirical calculations |
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