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Determination of uranium by thermal and epithermal neutron activation in natural waters and in human urine
Authors:Jiri Holzbecher  Douglas E Ryen
Institution:Trace Analysis Research Centre, Chemistry Department, Dalhousie University, Halifex, Nova Scotia B3H 4Jl Canada
Abstract:Uranium is determined via its 239U nuclide (74.0 keV, t12 = 23.5 min) in natural waters down to 0.03 ng U ml-1 after preconcentration with activated carbon and oxine; 30-min irradiation and counting times are used. No preconcentration is required for samples containing more than 4 ng U ml-1 with 10-min irradiation and counting times. Uranium in urine can be determined under a boron shield at the 5 ng ml-1 level after 30-min irradiation and counting.
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