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Asymmetric synthesis of S-5-benzyloxytryptophan,S-α-allylglycine and S-β-(2-naphthyl)alanine
Authors:Yu N Belokon'  N I Chernoglazova  E V Ivanova  A N Popkov  M B Saporovskaya  N N Suvorov  V M Belikov
Institution:(1) A. N. Nesmyanov Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, Moscow
Abstract:Conclusions The synthesis of optically pure S-5-benzyloxytryptophan, S-beta-(2-naphthyl)alanine, and S-agr-allylglycine was carried out by alkylating glycine in the Ni(II) complex of its Schiff base with S-2-N-(Nprime-benzylpropyl)aminobenzophenone, followed by Chromatographic separation of the mixture of diastereomeric alkylated complexes.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2818–2821, December, 1988.
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