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Pulsed laser induced synthesis of scheelite-type colloidal nanoparticles in liquid and the size distribution by nanoparticle tracking analysis |
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| Authors: | Jeong Ho Ryu Sin Young Bang Chang Sung Lim |
| Institution: | a Electro Materials & Device Center, Corporate R&D Institute, Samsung, Electro-Mechanics Co., Ltd., 314, Maetan 3-Dong, Yeongtong-Gu, Suwon-City, Guunggi-Do 443-743, South Korea b Division of Advanced Materials Science Engineering, Hanyang University, 17 Haengdang-Dong, Seongdong-Gu, Seoul 133-791, South Korea c Department of Advanced Materials Science and Engineering, Hanseo University, Seosan 356-706, South Korea |
| Abstract: | Pulsed laser ablation (PLA) of ceramic target in liquid phase was successfully employed to prepare calcium tungstate (CaWO4) and calcium molybdate (CaMoO4) colloidal nanoparticles. The crystalline phase, particle morphology and optical property of the colloidal nanoparticles were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and Raman spectroscopy. The produced stable colloidal suspensions consisted of the well-dispersed nanoparticles showing a spherical shape. The mechanism for the laser ablation and nanoparticle forming was discussed under consideration of photo-ablation process. Nanoparticle tracking analysis using optical microscope combined with image analysis was proposed to determine the size distribution function of the prepared colloidal nanoparticles. The mean size of the CaWO4 and CaMoO4 colloidal nanoparticles were 16 and 29 nm, with a standard deviations of 2.1 and 5.2 nm, respectively. |
| Keywords: | 42 62 &minus b 78 55 HX |
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