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新型碳基渗滤膜在易燃液体残留物提取检验中的应用
引用本文:杨瑞琴,段莉洁,谢文林.新型碳基渗滤膜在易燃液体残留物提取检验中的应用[J].分析试验室,2007,26(11):96-99.
作者姓名:杨瑞琴  段莉洁  谢文林
作者单位:1. 中国人民公安大学刑科技系,北京,100038
2. 长春工业大学化学系,长春,130054
3. 吉林省公安厅刑科所,长春,130051
摘    要:用自制的碳基渗滤膜,以自制的红外提取装置测定了该膜对苯的回收率为68%,考察了温度、压力、提取时间等对碳基渗滤膜应用的影响,主要介绍了将该碳基渗滤膜应用于现场易燃液体残留物的提取,通过水泥地面添加易燃液体的提取检验,棉布、化纤布上易燃液体残留物的提取检验测试了碳基渗透膜的提取回收能力.该碳基渗滤膜可以应用于纵火现场易燃液体残留物的提取检验.

关 键 词:碳基渗透膜  制备  应用  助燃剂
文章编号:1000-0720(2007)11-096-04
修稿时间:2006-06-07

The application of new carbon membrane in analysis of ignitable liquid residues
YANG Rui-qin,Duan Li-jie,XIE Wen-lin.The application of new carbon membrane in analysis of ignitable liquid residues[J].Chinese Journal of Analysis Laboratory,2007,26(11):96-99.
Authors:YANG Rui-qin  Duan Li-jie  XIE Wen-lin
Abstract:The application of the membrane in recovery of some popular arson accelerants such as gasoline, diesel, jet koresene and paint thinner, as well as their fire debris was studied in a laboratory recovery unit. About 68% benzene spiked in the cement could be recovered within 20 rain under 100 ~C. High temperature and vacuum conditions were beneficial to recovering fire accelerants and debris from spiked cements. With the membrane and recovery method, the gasoline, diesel, and paint thinner in the cement were satisfactorily recovered and were then separated and analyzed on GC-FID. The gasoline, diesel, jet koresene and paint thinner spiked in the carpet and cotton, were recovered together with their fire debris by using this membrane, and were analyzed on GC-FID.
Keywords:Carbon membrane  Application  Fire debris
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