Synthesis and transformations of 1-(azidophenyl)-1H-tetrazoles |
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Authors: | N. T. Pokhodylo V. S. Matiichuk N. D. Obushak |
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Affiliation: | 1. Ivan Franko Lviv National University, ul. Kirilla i Mefodiya 6, Lviv, 79005, Ukraine
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Abstract: | Diazotization of 1-(aminophenyl)-1H-tetrazoles and subsequent treatment of the diazonium salts with sodium azide gave 1-(azidophenyl)-1H-tetrazoles which were brought into cyclization with ethyl acetoacetate and cyanoacetanilide to obtain 1,2,3-triazole derivatives. Under these conditions, the tetrazole ring may undergo cleavage with formation of cyanamide group. |
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