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Potassium decamolybdodiferrate(III): Synthesis and characterization
Authors:G K Kaziev  A V Oreshkina  S Holguin Quinones  A A Kanaev  T Yu Galzunova
Institution:(1) Moscow State Pedagogical University, Malaya Pirogovskaya ul. 1, Moscow, 119882, Russia;(2) Universidad Autonoma Metropolitana Azcapotzalco, Mexico, Russia;(3) Moscow State University, Vorob’evy gory, Moscow, 119992, Russia
Abstract:Potassium decamolybdodiferrate(III) of composition K6Fe2Mo10O34(OH)4] · 7H2O (compound I) is synthesized and characterized by IR spectroscopy, thermogravimetry, and powder X-ray diffraction. The crystals of compound I are monoclinic with a = 9.7482 Å, b = 6.5663 Å, c = 7.8453 Å, β = 116.81°, V = 448.15 Å3, ρ = 3.115 g/cm3.
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