New deprotection method of the 2,2,2-trichloroethoxycarbonyl (Troc) group with (Bu3Sn)2 |
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| Authors: | Hiroomi Tokimoto |
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| Institution: | Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka 560-0043, Japan |
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| Abstract: | The 2,2,2-trichloroethoxycarbonyl (Troc) group was efficiently removed in high yields with (Bu3Sn)2 in DMF under microwave heating. The present method was applied to deprotection of the Troc group on solid support. |
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| Keywords: | Protective group Deprotection Radical reaction Microwave |
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