Comparison of atomic absorption,mass and X-ray spectrometry techniques using dissolution-based and solid sampling methods for the determination of silver in polymeric samples |
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Authors: | Isabel De Schrijver Maite Aramendia Laszlo Vincze Martín Resano Ann Dumoulin Frank Vanhaecke |
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Institution: | 1. Ghent University, Department of Analytical Chemistry, Krijgslaan 281-S12, B-9000 Ghent, Belgium;2. University College West-Flanders, Department of Industrial Engineering and Technology, Research group EnBiChem, Graaf Karel de Goedelaan 5, B-8500 Kortrijk, Belgium;3. University of Zaragoza, Department of Analytical Chemistry, Pedro Cerbuna 12, E-50009 Zaragoza, Spain |
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Abstract: | In this work, the capabilities and limitations of solid sampling techniques – laser ablation inductively coupled plasma mass spectrometry (LA-ICPMS), wavelength dispersive X-ray fluorescence spectrometry (WD-XRFS) and solid sampling electrothermal atomic absorption spectrometry (SS-ETAAS) – for the determination of silver in polymers have been evaluated and compared to those of acid digestion and subsequent Ag determination using pneumatic nebulization ICPMS (PN-ICPMS) or flame AAS (FAAS). |
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Keywords: | ICPMS AAS XRFS Solid sampling Silver determination |
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