| 乙二胺溶剂热还原法制备碳纳米管 |
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| 引用本文： | 米远祝,刘应亮,袁定胜,张静娴,肖勇. 乙二胺溶剂热还原法制备碳纳米管[J]. 广州化学, 2005, 30(1): 1-4 |
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| 作者姓名： | 米远祝 刘应亮 袁定胜 张静娴 肖勇 |
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| 作者单位： | 暨南大学,化学系,广东,广州,510632;湖北民族学院,化工系,湖北,恩施,445000;暨南大学,化学系,广东,广州,510632 |
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| 基金项目： | 广东省教育厅“千百十人才工程”资助项目(Q02059)，广东省科技计划资助项目(2KM02304G) |
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| 摘 要： | 以乙二胺作为溶剂和碳源,用KBH4还原NiCl2得到的镍作为催化剂,于300℃制备碳纳米管。X-射线衍射(XRD)、透射电子显微镜(TEM)、选区电子衍射(SAED)和Raman光谱分析证明,产品为多壁碳纳米管,直径约为100nm,长度达几微米。该方法具有反应温度低、反应时间短、操作简便等特点。
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| 关 键 词： | 乙二胺 溶剂热还原 碳纳米管 |
| 文章编号： | 1009-220X(2004)04-0001-04 |
| 修稿时间： | 2004-08-25 |
Synthesis of carbon nanotubes via ethylenediamine-thermal reduction route |
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| MI Yuan-zhu,LIU Ying-liang,YUAN Ding-sheng,ZHANG Jing-xian,XIAO Yong. Synthesis of carbon nanotubes via ethylenediamine-thermal reduction route[J]. Guangzhou Chemistry, 2005, 30(1): 1-4 |
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| Authors: | MI Yuan-zhu LIU Ying-liang YUAN Ding-sheng ZHANG Jing-xian XIAO Yong |
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| Affiliation: | MI Yuan-zhu1,2,LIU Ying-liang1*,YUAN Ding-sheng1,ZHANG Jing-xian1,XIAO Yong1 |
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| Abstract: | Carbon nanotubes were prepared using KBH4 and NiCl2 as staring materials and using ethylenediamine as carbon sources and solvent. The products were characterized with X-ray powder diffractometer(XRD),transmission electronic microscopy(TEM),selected-area electron diffraction(SAED)and Raman spectroscopy. The results showed that the products were hexaganol phase canbon nanotubes with the average diameter of 100 nm and the length of several microns. |
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| Keywords: | ethylenediamine solvothermal carbon nanotubes |
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