| 羟基功能化离子液体中Pd纳米微粒制备与结构表征 |
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| 引用本文： | 代 闯,张晟卯,李 健,吴志申,张治军.羟基功能化离子液体中Pd纳米微粒制备与结构表征[J].无机化学学报,2007,23(9):1653-1656. |
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| 作者姓名： | 代 闯 张晟卯 李 健 吴志申 张治军 |
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| 作者单位： | 1. 河南大学特种功能材料重点实验室,开封,475004
2. 河南大学特种功能材料重点实验室,开封,475004;中国科学院兰州化学物理研究所固体润滑国家重点实验室,兰州,730000 |
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| 基金项目： | 国家自然科学基金;河南省自然科学基金 |
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| 摘 要： | 1-Ethoxyl-3-methyl imidazolium tetrafluoroborate (C2OHmim]BF4)， 1-(4′-hydroxyl)-butyl-3-methyl imidazolium tetrafluoroborate (C4OHmim]BF4) and 1-(6′-hydroxyl)-hexyl-3-methyl imidazolium tetrafluoroborate(C6OHmim]BF4) were synthesized and then Pd nanoparticles were prepareds in these ionic liquids .The structure and shape of Pd nanoparticles were investigated by XRD and TEM. The results indicate that the Pd nanoparticles are fcc structure and there are some differences in the diameter of Pd nanoparticles prepared in different ionic liquids， i.e. 150 nm， 30 nm， 10 nm， respectively. The formation mechanism of nanoparticles is proposed.
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| 关 键 词： | 羟基功能化离子液体 Pd纳米微粒 形成机理 |
| 文章编号： | 1001-4861（2007）09-1653-04 |
| 修稿时间： | 2007-05-08 |
Preparation and Structure Characterization of Pd Nanoparticles in Hydroxyl-functionalized Ionic Liquids |
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| DAI Chuang,ZHANG Sheng-Mao,LI Jian,WU Zhi-Shen and ZHANG Zhi-Jun.Preparation and Structure Characterization of Pd Nanoparticles in Hydroxyl-functionalized Ionic Liquids[J].Chinese Journal of Inorganic Chemistry,2007,23(9):1653-1656. |
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| Authors: | DAI Chuang ZHANG Sheng-Mao LI Jian WU Zhi-Shen and ZHANG Zhi-Jun |
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| Institution: | 1.Special Functional Material Laboratory, Henan University, Kaifeng, Henan 475001;2.State Key Laboratory of Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000 |
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| Abstract: | |
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| Keywords: | Hydroxyl-functionalized ionic liquids Pd nanoparticles formation mechanism |
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