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Determination of the sodium-to-calcium ratio in sections of undecalcified bone tissue by neutron activation analysis
Authors:M. Rakovič  J. Kučera  N. Pilecká  C. Povyšil
Affiliation:(1) Institute of Biophysics, 1st Medical Faculty, Charles University, Salmovská 3, 120 00 Prague 2, "Ccaron"SFR;(2) Nuclear Research Institute, 250 68 "Rcaron"e"zcaron" near Prague, "Ccaron"SFR;(3) 2nd Institute of Pathology, 1st Medical Faculty, Charles University, Prague, "Ccaron"SFR
Abstract:The feasibility has been shown of instrumental determination of the Na/Ca ratio with a standard deviation of 4.7% in sections of undecalcified bone tissue made from standard biopsy or autopsy bone samples (about 0.5 mg in weight) embedded in poly (methyl methacrylate) blocks. The determination was based on short-time activation and counting the24Na and49Ca radionuclides. Blank values and detection limits of the elements were evaluated and possibilities to detect changes of the Na/Ca ratio are discussed.
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