| 血、肝、尿中地西泮等4种药物的固相萃取-紫外导数光谱检测法 |
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| 引用本文： | 谭家镒,姜兆林,吴玉红.血、肝、尿中地西泮等4种药物的固相萃取-紫外导数光谱检测法[J].分析化学,1999,27(11):1317-1319. |
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| 作者姓名： | 谭家镒 姜兆林 吴玉红 |
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| 作者单位： | 中国刑警学院法医系,沈阳,110035 |
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| 摘 要： | 血，肝，尿中地西泮，去甲西泮，替马西泮及奥沙西泮用ＧＤＸ３０１大孔树脂萃取，萃取物制成酸性水溶液测定二阶导数光谱，方法简便快速。血和尿中４种药物的提取率近似为１００％，检出限近似为０．８ｍｇ／Ｌ；肝中４种药物的最以率近似为８０％，检出限近似为１．２μｇ／ｇ。
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| 关 键 词： | 地西泮 去甲西泮 替马西泮 奥沙西泮 固相萃取 紫外导数光谱法 生物检材 |
The Determination of Diazepam, Nordiazepam, Temazepam and Oxazepam in Blood, Liver and Urine by Solid-phase Extraction and Derivative Ultraviolet Spectrophotometry |
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| Tan Jiayi,Jiang Zhaolin,Wu Yuhong.The Determination of Diazepam, Nordiazepam, Temazepam and Oxazepam in Blood, Liver and Urine by Solid-phase Extraction and Derivative Ultraviolet Spectrophotometry[J].Chinese Journal of Analytical Chemistry,1999,27(11):1317-1319. |
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| Authors: | Tan Jiayi Jiang Zhaolin Wu Yuhong |
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| Abstract: | |
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| Keywords: | Diazepam nordiazepare temazepam oxazepam biological sample solid-phase extraction derivative ultraviolet spectrophotometry |
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