Thermal behaviour of thallium(I) fatty acid salts,II |
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Authors: | T Meisel K Seybold J Róth |
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Institution: | (1) Institute for General and Analytical Chemistry, Technical University of Budapest, Hungary |
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Abstract: | The electrical conductivity (EC) changes of thallium(I) salts of fatty acids, which possess liquid crystalline phases, were investigated as a function of temperature. It was found that sharp EC jumps are associated with the phase transitions. The EC of the liquid crystalline phases depended not only on the temperature, the molecular weight and the geometry of the measuring cell, but also very sensitively on the heat treatment conditions which affect the relative magnitude of the EC in the mesophases.Study of these dependences revealed a memory effect . An explanation is given for this phenomenon.
Zusammenfassung Die Änderungen der elektrischen Leitfähigkeit (EC) von Fettsäure-Thalium(I)-Salzen mit flüssig-kristallinen Phasen wurden als Funktion der Temperatur untersucht. Es wurde festgestellt, daß den Phasenübergängen scharfe EC-Sprünge entsprechen. Die EC der flüssig-kristallinen Phase hängt nicht nur von der Temperatur, dem Molekulargewicht und der Geometrie der Meßzelle ab, sondern auch — in sehr empfindlicher Weise — Phasen bestimmen.Die Untersuchung dieser Zusammenhänge führte zur Beobachtung eines »Memorieeffektes« Eine Erklärung dieser Erscheinung wird gegeben.
Résumé On a étudié les variations de la conductibilité électrique (EC) des sels de thallium(I) des acides gras possédant des phases cristallines liquides, en fonction de la température. On a établi que les variations brusques d'EC correspondent aux transitions de phases. L'EC des phases cristallines liquides dépend non seulement de la température, de la masse molaire et de la géométrie de la cellule de mesure, mais aussi, et d'une manière très sensible, des conditions du traitement thermique qui affectent l'amplitude relative de l'EC dans les mésophases.Un «effet de mémoire» a été observé lors de l'étude de ces phénomènes, dont on donne une explication.
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![ecy](/content/x8h13688k7396755/xxlarge1101.gif) ![tcy](/content/x8h13688k7396755/xxlarge1090.gif) ![ocy](/content/x8h13688k7396755/xxlarge1086.gif) ![mcy](/content/x8h13688k7396755/xxlarge1084.gif) ![yacy](/content/x8h13688k7396755/xxlarge1103.gif) ![vcy](/content/x8h13688k7396755/xxlarge1074.gif) ![iecy](/content/x8h13688k7396755/xxlarge1077.gif) ![ncy](/content/x8h13688k7396755/xxlarge1085.gif) ![icy](/content/x8h13688k7396755/xxlarge1080.gif) .
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