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Synthesis of high‐aspect‐ratio,top‐open and ultraflat‐surface TiO2 nanotubes through double‐layered configuration
Authors:Jia Lin  Xianfeng Chen
Affiliation:Department of Physics, The State Key Laboratory on Fiber Optic Local Area Communication Networks and Advanced Optical Communication Systems, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P.R. China
Abstract:In this Letter, a novel modified anodization was utilized to synthesize high‐aspect‐ratio, top‐open and ultraflat‐surface TiO2 nanotubes. The interruption of voltage during anodization leads to the formation of a double‐layered structure. Due to the weak mechanical connection between the upper and the underlying layer, the two parts can be easily detached. Compared with the conventional ultrasonication method to remove the clusters of nanotubes where rough surfaces resulted, this efficient and reliable strategy may facilitate further applications of TiO2 nanotubes in diverse conditions.
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Keywords:TiO2  nanotubes  surface disorder  double layers  ultraflat surfaces
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