| Abstract: | The crystal structure of 4-trimethyltin-quinuclidinium perchlorate has been determined by direct methods and refined by least squares techniques. Crystals of C10H22ClNO4Sn are monoclinic, space group I2/c with lattice parameters a = 29.445 (13), b = 18.400(8), c = 11.300(5) Å, β = 95.82(5)°, V = 6090.65Å3, and two independent molecules (Z = 16), Interatomic distances are compared with those of known structures of quinuclidinium chloride and 4-haloquinuclidinium chlorides and perchlorates. |
