Abstract: | A method for quantitative characterization of the noncrystalline region in poly(ethylene terephthalate) (PET) fibers based on x-ray wide-angle diffraction data is elaborated. The procedure consists in a computational resolution of the diffracted intensity into individual peaks for 010, 11 0, and 100 planes and into isotropic and anisotropic components of diffuse scattering. The results show that the content of mesomorphic regions in the noncrystalline part of PET fibers with draw ratio of λ = 3.0 varies from 12% to 32% depending on the temperature of heat treatment. |