A selective method for the determination of benzo[a]pyrene in soil using porous graphitic carbon liquid chromatography columns |
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Authors: | Al-Haddad Ameera |
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Institution: | Department of Chemistry, University of Bahrain, P.O. Box 32038, Isa Town, Bahrain |
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Abstract: | A back-flushing procedure using porous graphitic carbon (PGC) HPLC columns has been used successfully for the cleanup of soil samples for the determination of benzoa]pyrene in ppb levels by an ODS-fluorescence HPLC column. The procedure was tested on nine random soil samples taken from an industrial area of the Kingdom of Bahrain. The mean percent recovery from the PGC column was 96% and the average coefficient of variation for the whole method was 5.2%. |
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Keywords: | Benzo[a]pyrene Porous graphitic carbon Soil analysis Polycyclic aromatic hydrocarbons |
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