| 盐酸法测定γ-(2.3环氧丙氧)丙基三甲氧基硅烷偶联剂 |
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| 引用本文： | 李德亮,常志显,徐翔民,吴志申,张治军.盐酸法测定γ-(2.3环氧丙氧)丙基三甲氧基硅烷偶联剂[J].河南大学学报(自然科学版),2007,37(1):42-45. |
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| 作者姓名： | 李德亮 常志显 徐翔民 吴志申 张治军 |
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| 作者单位： | 河南大学,特种功能材料重点实验室,河南,开封,475001;河南大学,化学化工学院,河南,开封,475001;河南大学,化学化工学院,河南,开封,475001;河南大学,特种功能材料重点实验室,河南,开封,475001 |
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| 摘 要： | 建立了滴定分析测定γ-(2.3环氧丙氧)丙基三甲氧基硅烷偶联剂的新方法,探讨了反应用酸、溶剂、HCl浓度、放置时间、指示剂等因素对测定结果的影响.其样品的回收率为100.3%~101.1%,相对标准偏差0.37%.
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| 关 键 词： | γ-(2.3环氧丙氧)丙基三甲氧基硅硅烷 滴定 盐酸 丁酮 |
| 文章编号： | 1003-4978（2007）01-0042-04 |
| 修稿时间： | 2006-09-16 |
Determination of Gamma-glycidoxypropyltrimethoxysilane with HCl |
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| LI De-liang,CHANG Zhi-xian,XU Xiang-min,WU Zhi-shen,ZHANG Zhi-jun.Determination of Gamma-glycidoxypropyltrimethoxysilane with HCl[J].Journal of Henan University(Natural Science),2007,37(1):42-45. |
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| Authors: | LI De-liang CHANG Zhi-xian XU Xiang-min WU Zhi-shen ZHANG Zhi-jun |
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| Institution: | 1. Key Laboratory for Special Functional Materials, Henan University, Henan Kai feng 475001, China; 2. Department of Chemistry and Chemical Engineering , Henan University, Henan Kai feng 475001, China |
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| Abstract: | Determination of glycidoxypropyltrimethoxysilane with titrate method is established.The influences of different acids,solvents,HCl concentration,reacting time and indicator have been researched,and the result is satisfactory.The sample recovery and the relative standard deviation are 100.3%~101.1% and 0.37%,respectively. |
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| Keywords: | glycidoxypropyltrimethoxysilane titration hydrochloric acid butanone |
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