Synthesis and characterization of complexes of UO2(II) and Th(IV) of bis-schiff bases derived from furoylpyrazolone |
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| Authors: | G. X. Zheng Q. F. Wang S. G. Luo |
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| Affiliation: | (1) Department of Chemical Engineering, Jinan University, Jinan, 250022, P.R. China;(2) China Institute of Atomic Energy, Beijing, 102413, P.R. China |
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| Abstract: | Four new complexes of UO2(II) and Th(IV) with bis-Schiff bases, derived from N,N'-bis[(l-phenyl-3-methyl-5-oxo-4-pyrazolinyl)-a-furylmethylidyne]-1,2-propylenediimine [1,2-BPMOPFP-H2] and N,N'- bis[(l-phenyl-3-methyl-5-oxo-4-pyrazolinyl)-a-furylmethylidyne]-1,3-propylenediimine [1,3-BPMOPFP-H2], were synthesized and characterized by elemental analysis, IR, UV, 1HNMR spectroscopy, and molar conductivity. The general formula of the complexes was confirmed to be [UO2(BPMOPFP)], [Th(BPMOPFP)(NO3)]NO3. A possible structure for the complexes have been proposed. |
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