Separation of titanium, iron and aluminium on a chelating resin with benzoylphenylhydroxylamine group and application to bauxite and clay |
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Authors: | Jyotirmoy Das and Maya Pobi |
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Affiliation: | (1) Department of Chemistry, University of Burdwan, 713104 Burdwan, India |
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Abstract: | Summary A chelating polystyrene based resin containing N-benzoyl-N-phenylhydroxylamine has been sythesized by two methods and characterized. Conditions for quantitative separation of Ti(IV), Fe(III) and Al(III) on the resin have been studied. A method has been developed for the determination of these three metal ions in bauxite or clay samples after their separation on the resin with recoveries of 98.5–99.5% for different metal ions. The maximum sorption values are observed at pH 1, 2.5 and 2.5 for Ti(IV), Fe(III) and Al(III), respectively, which are recovered by successive elution with 1 mol/l H2SO4, 2 mol/l HCl and 4 mol/l H2SO4 in the above order. |
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