| 工业混合烷中含硫化合物的鉴定 |
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| 引用本文： | 窦云芹,高岩,于淑杰,李晓丽,宋会美,张立超,曹帼英,谷晓庆,李铁纯,汪子明,张寒琦.工业混合烷中含硫化合物的鉴定[J].应用化学,2009,26(8):993-995. |
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| 作者姓名： | 窦云芹 高岩 于淑杰 李晓丽 宋会美 张立超 曹帼英 谷晓庆 李铁纯 汪子明 张寒琦 |
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| 作者单位： | (1.大庆油田化工有限公司技术开发研究院分析检测中心 大庆；2.大庆油田化工有限公司 大庆；;
3.鞍山师范学院化学系 鞍山；4.吉林大学化学学院 长春 130012) |
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| 摘 要： | 建立了一种工业混合烷中含硫化合物的新的定性鉴定方法。样品经过氢氧化钾和硝酸银预处理后，可将工业混合烷中含硫化合物的硫醇、硫醚和噻吩进行分离，而后用GC-MS测定，鉴定了工业混合烷中30种硫醚和5种硫醇化合物。
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| 关 键 词： | 工业混合烷 硫醇 硫醚 |
| 收稿时间： | 2008-08-04 |
| 修稿时间： | 2009-02-17 |
Identify of the sulfur compounds in industrial mixed alkanes |
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| DOU Yun-Qin,GAO Yan,YU Shu-Jie,LI Xiao-Li,SONG Hui-Mei,ZHANG Li-Chao,CAO Guo-Ying,GU Xiao-Qing,LI Tie-Chun,WANG Zi-Ming,ZHANG Han-Qi.Identify of the sulfur compounds in industrial mixed alkanes[J].Chinese Journal of Applied Chemistry,2009,26(8):993-995. |
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| Authors: | DOU Yun-Qin GAO Yan YU Shu-Jie LI Xiao-Li SONG Hui-Mei ZHANG Li-Chao CAO Guo-Ying GU Xiao-Qing LI Tie-Chun WANG Zi-Ming ZHANG Han-Qi |
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| Institution: | (1.Analytical Center,Research Institute of Technology Development,Chemical Engineering ;
and Technology Corporation of Daqing Oil Field,Daqing;
2.Daqing Oil Field,Daqing; 3.College of Chemistry,Anshan Normal College,Anshan;;
4.College of Chemistry,Jilin University,Changchun 130012) |
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| Abstract: | In the paper, a method for identifying the sulfur compounds in industrial mixed alkanes was developed. By treating samples with KOH and AgNO3, mercaptan, thioether and thiophene were separated and enriched effectively from industrial mixed alkanes, which were in favor of the analysis by GC-MS. 30 kinds of thioether compounds and 5 kinds of mercaptan compounds in industrial mixed alkanes were detectable. |
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| Keywords: | Industrial mixed alkanes thioether mercaptan |
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