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Continuous-flow synthesis of activated vitamin D3 and its analogues
Authors:Fuse Shinichiro  Mifune Yuto  Tanabe Nobutake  Takahashi Takashi
Affiliation:Department of Applied Chemistry, Tokyo Institute of Technology, 2-12-1, Ookayama, Tokyo 152-8552, Japan.
Abstract:An efficient, two-stage, continuous-flow synthesis of 1α,25-(OH)(2)-vitamin D(3) (activated vitamin D(3)) and its analogues was achieved. The developed method afforded the desired products in satisfactory yields using a high-intensity and economical light source, i.e., a high-pressure mercury lamp. In addition, our method required neither intermediate purification nor high-dilution conditions.
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