Synthesis of the first 2,3-dihydro-1,2,3-azadiphosphete complex |
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Authors: | Ionescu E Jones P G Streubel R |
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Affiliation: | Institut für Anorganische und Analytische Chemie der Technischen Universit?t Braunschweig, Postfach 3329, D-38023 Braunschweig, Germany. |
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Abstract: | Synthesis of the first 2,3-dihydro-1,2,3-azadiphosphete complex was achieved via thermal reaction of a 2H-azaphosphirene complex in o-xylene, whereby a 2,5-dihydro-1,3-diaza-2,5-diphosphinine complex and a further unidentified byproduct were formed; the structure of the title compound was established through an X-ray single-crystal diffraction study. |
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