Development and application of combinatorial electrostatic atomization system “M-ist Combi”: High-throughput preparation of electrode materials |
| |
| Institution: | 1. Department of Pure and Applied Chemistry, Faculty of Science and Technology, Tokyo University of Science, 2641 Yamazaki, Noda, Chiba 278-8510, Japan;2. Applied Materials Laboratory, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044, Japan;3. National Institute for Materials Science, 1-2-1 Sengen, Tsukuba, Ibaraki 305-0047, Japan;1. Department of Chemical Engineering, National Taiwan University, Taipei, Taiwan, ROC;2. Sino-American Silicon Productions Inc., Hsin-chu, Taiwan, ROC;1. Department of Electronics, College of Electronic Information and Optical Engineering, Nankai University, Tianjin 300071, PR China;2. Department of Physics, University of Puerto Rico Rio Piedras, San Juan, PR 00931, USA;1. Institute of Physics, University of Silesia, ul. Uniwersytecka 4, 40-007 Katowice, Poland;2. Department of Inorganic and Analytical Chemistry, West Pomeranian University of Technology, Al. Piastów 42, 71-065 Szczecin, Poland;1. State Key Laboratory for Mechanical Behavior of Materials, Xi''an Jiaotong University, Xi''an 710049, China;2. School of Microelectronics, Xi''an Jiaotong University, Xi''an 710049, China |
| |
| Abstract: | We introduce a newly developed combinatorial electrostatic atomization system, “M-ist Combi,” and demonstrate the effectiveness of the system by establishing a pseudo-ternary Li–Ni–Co oxide phase diagram. After heating the starting materials with compositions in the range of 0.4 ≤ Li / (Li + Ni + Co) ≤ 0.6 at 973 K for 3 h, the diffraction of all of the products was indexed as single-phase with layer-type hexagonal structures such as LiCoO2 and LiNiO2. As the substitution quantity of Co to the Ni site increased, the value of 2θ shifted to a high-angle. By combining the M-ist Combi system with combinatorial XRD apparatus, we successfully completed the high-throughput sample preparation and phase identification of over 150 samples in one day. |
| |
| Keywords: | |
| 本文献已被 ScienceDirect 等数据库收录！ |
|
