| 微波辅助-原子吸收光谱法测定翻白草中的铜与铁 |
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| 引用本文： | 黄露,陈毅挺,林棋,张振华. 微波辅助-原子吸收光谱法测定翻白草中的铜与铁[J]. 光谱实验室, 2011, 28(6): 3265-3267 |
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| 作者姓名： | 黄露 陈毅挺 林棋 张振华 |
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| 作者单位： | 闽江学院化学与化学工程系 福州市闽侯上街大学城文贤路1号350108 |
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| 基金项目： | 福建省青年人才创新项目(2010J05029); 福建省教育厅科技项目(JA10222,JB09188,JB11142) |
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| 摘 要： | 利用微波萃取法进行提取,以稀盐酸为提取剂,浓硝酸-高氯酸为消解体系,采用原子吸收光谱法测定翻白草中铁和铜的含量.翻白草铜、铁元素的提取时间均为150s,阳极电流为120mA,料液比为1:20(g/mL),铜、铁提取剂酸度分别为1.5和1.0.翻白草根中铜的溶出量最大,而叶中铁的溶出量最大.
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| 关 键 词： | 翻白草 微波萃取 原子吸收光谱法 铁 铜 |
Determination of Copper and Iron in Potentilla Discolor by Atomic Absorption Spectrometry with Microwave Assisted |
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| HUANG Lu,CHEN Yi-Ting,LIN Qi,ZHANG Zhen-Hua. Determination of Copper and Iron in Potentilla Discolor by Atomic Absorption Spectrometry with Microwave Assisted[J]. Chinese Journal of Spectroscopy Laboratory, 2011, 28(6): 3265-3267 |
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| Authors: | HUANG Lu CHEN Yi-Ting LIN Qi ZHANG Zhen-Hua |
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| Affiliation: | HUANG Lu CHEN Yi-Ting LIN Qi ZHANG Zhen-Hua(Department of Chemistry and Chemical Engineering,Minjiang University,Fuzhou 350108,P.R.China) |
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| Abstract: | The samples were extracted by microwave extraction with diluted hydrochloric acid as extractant and concentrated nitric acid-perchloric acid as digestion system,and the contents of copper and iron in potentilla discolor were determined by atomic absorption spectrophotometry（AAS）.The extraction time for both copper and iron was 150s,and the anode current was 120mA,and the solid-liquid ratio was 1∶20（g/mL）;and the acidities of the extractants for copper and iron were 1.5 and 1.0,respectively.The highest release amount of copper was found in the roots of potentilla discolor,while that of iron was found in the leaves. |
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| Keywords: | Potentilla Discolor Microwave Extraction AAS Iron Copper |
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