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汉中元胡中8种金属元素含量的测定
引用本文:孙妩娟.汉中元胡中8种金属元素含量的测定[J].光谱实验室,2011,28(6):2987-2990.
作者姓名:孙妩娟
作者单位:陕西理工学院化学与环境科学学院 陕西省汉中市朝阳路附1号723001
基金项目:陕西理工学院校级项目(SLG0912)
摘    要:采用微波消解-火焰原子吸收光谱法对汉中元胡中钾、钙、钠、镁、锌、锰、铜、铁8种金属元素的含量进行测试,测得结果分别为K(2033.97mg/kg)、Ca(600.87mg/kg)、Na(1395.55 mg/kg)、Mg(494.88mg/kg)、Zn(220.36mg/kg)、Mn(107.75mg/kg)、Cu(39.68mg/kg)、Fe(2462.79mg/kg)。相对标准偏差的范围为0.0356%—4.4288%,回收率的范围为96.8%—101.2%。微波消解-火焰原子吸收光谱法是一种简便而又灵敏的测定中草药中微量元素的方法。

关 键 词:元胡  微量元素  微波消解  原子吸收光谱法

Determination of Eight Metal Elements in Corydalis Sample from Hanzhong
SUN Wu-Juan.Determination of Eight Metal Elements in Corydalis Sample from Hanzhong[J].Chinese Journal of Spectroscopy Laboratory,2011,28(6):2987-2990.
Authors:SUN Wu-Juan
Institution:SUN Wu-Juan(College of Chemistry and Environment Science,Shaanxi University of Technology,Hanzhong,Shaanxi 723000,P.R.China)
Abstract:Eight metal elements such as potassium,calcium,sodium,magnesium,zinc,manganese,iron and copper from hanzhong corydalis sample were determined by FAAS with microwave digestion.The concentration of potassium,calcium,sodium,magnesium,zinc,manganese,copper and iron were 2033.97,600.87,1395.55,494.88,220.36,107.75,39.68mg/kg and 2462.79mg/kg,respectively.The relative standard deviations were 0.0356%—4.4288% and average recovery were 96.8%—101.2%.This method is simple and sensitive for determination of trace elements from medicinal herbs.
Keywords:Corydalis  Trace Element  Microwave Digestion  AAS  
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