| 高比表面积有序介孔碳的制备及光谱表征 |
| |
| 引用本文： | 游波,杨俊,谢卫,黄朝章,许寒春,刘泽春,苏庆德.高比表面积有序介孔碳的制备及光谱表征[J].光谱实验室,2011,28(6):3113-3116. |
| |
| 作者姓名： | 游波 杨俊 谢卫 黄朝章 许寒春 刘泽春 苏庆德 |
| |
| 作者单位： | 1. 中国科学技术大学烟草与健康研究中心 合肥市徽州大道1129号230052
2. 福建中烟工业公司技术中心 福建省厦门市海沧新阳工业区新阳路1号361022 |
| |
| 基金项目： | 福建中烟工业公司科技项目(20090914) |
| |
| 摘 要： | 以酚醛树脂低聚物为有机前驱体、正硅酸四乙酯(TEOS)为无机前驱体、嵌段共聚物F127为模板,采用蒸发诱导三组分共组装的方法合成了具有高比表面积的有序介孔碳材料.利用X射线衍射仪(XRD)、透射电子显微镜(TEM)、傅里叶变换红外光谱仪(FTIR)、拉曼光谱仪(Raman)、氮气吸附脱附仪对该材料的组成、结构及形貌等进...
|
| 关 键 词： | 三组分 介孔碳 表征 自组装 |
Preparation and Spectroscopic Characterization of Ordered Mesoporous Carbon with High Specific Surface Areas |
| |
| YOU Bo,YANG Jun,XIE Wei,HUANG Chao-Zhang,XU Han-Chun,LIU Ze-Chun,SU Qing-De.Preparation and Spectroscopic Characterization of Ordered Mesoporous Carbon with High Specific Surface Areas[J].Chinese Journal of Spectroscopy Laboratory,2011,28(6):3113-3116. |
| |
| Authors: | YOU Bo YANG Jun XIE Wei HUANG Chao-Zhang XU Han-Chun LIU Ze-Chun SU Qing-De |
| |
| Institution: | YOU Bo YANG Jun XIE Weia HUANG Chao-Zhanga XU Han-Chuna LIU Ze-Chuna SU Qing-De(Research Center of Tobacco and Health,University of Science and Technology of China,Hefei 230052,P.R.China)a(Technical Center of Fujian Tobacco Industry Corporation,Xiamen,Fujian 361022,P.R.China) |
| |
| Abstract: | Ordered mesoporous carbons with high specific surface areas were prepared by evaporation induced triconstituent co-assembly method,with phenolic resin oligomers as organic precursor,tetraethyl orthosilicate(TEOS) as inorganic precursor and segmented copolymer F127 as template.The composition,structure and morphology of the prepared samples were characterized by XRD,TEM,FTIR,Raman and N2 sorption techniques.The prepared ordered mesoporous carbons had highly ordered two dimension-hexagonal mesostructured with... |
| |
| Keywords: | Triconstituent Mesoporous Carbon Characterization Self-Assembly |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
