| 直接测汞仪测定涂料中的总汞 |
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| 引用本文： | 宋保靓,李彬,余淑媛,刘志红,吴景武,王宏菊,任聪,冯均利,邹春海. 直接测汞仪测定涂料中的总汞[J]. 光谱实验室, 2011, 28(5): 2444-2447 |
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| 作者姓名： | 宋保靓 李彬 余淑媛 刘志红 吴景武 王宏菊 任聪 冯均利 邹春海 |
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| 作者单位： | 深圳出入境检验检疫局 广东省深圳市福田区福强路1011号518045 |
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| 基金项目： | 国家质检总局标准项目(2009B080) |
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| 摘 要： | 采用直接测汞仪对涂料样品进行了总汞含量的分析测定。通过正交试验法对干燥温度、干燥时间、分解温度、分解时间等条件进行了优化,并进行了线性关系、精密度、回收率等实验。结果表明,本方法线性范围5—500ng,相关系数≥0.9994,检出限为0.024ng,回收率在97.0%—108.5%之间,相对标准偏差小于5.4%。本方法灵敏度高,简便、快速、准确,适用于对涂料中的总汞的测定。
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| 关 键 词： | 汞 直接测汞仪 涂料 正交试验 |
Determination of Total Mercury in Paint by Direct Mercury Analyzer |
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| SONG Bao-Liang,LI Bin,YU Shu-Yuan,LIU Zhi-Hong,WU Jing-Wu,WANG Hong-Ju,REN Cong,FENG Jun-Li,ZOU Chun-Hai. Determination of Total Mercury in Paint by Direct Mercury Analyzer[J]. Chinese Journal of Spectroscopy Laboratory, 2011, 28(5): 2444-2447 |
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| Authors: | SONG Bao-Liang LI Bin YU Shu-Yuan LIU Zhi-Hong WU Jing-Wu WANG Hong-Ju REN Cong FENG Jun-Li ZOU Chun-Hai |
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| Affiliation: | SONG Bao-Liang LI Bin YU Shu-Yuan LIU Zhi-Hong WU Jing-Wu WANG Hong-JuREN Cong FENG Jun-Li ZOU Chun-Hai(Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen,Guangdong 518045,P.R.China) |
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| Abstract: | The quantitative analysis of total mercury in paint was established by direct mercury analyzer.The conditions,such as drying temperature,drying time,decomposition temperature and decomposition time,were optimized by orthogonal experiment.Under optimal conditions,good linear correlation,recovery and precision were obtained.The linearity range of the method was 5—500ng,the correlation coefficient was greater than or equal to 0.9994,the detection limit was 0.024ng,the recvoeries were 97.0%—108.5% and the relative standard deviations were less than 5.4%.The method is simple,sensitive and accurate,and that is suit to apply to the determination of total mercury in paint. |
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| Keywords: | Mercury Direct Mercury Analyzer Paint Orthogonal Experiment |
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