Synthesis and Characterization of Ag2S Nanocrystals in Hyperbranched Polyurethane at Room Temperature |
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Authors: | S.H. LiuX.F. Qian J. YinL. Hong X.L. WangZ.K. Zhu |
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Affiliation: | Research Institute of Polymer Materials, School of Chemistry and Chemical Technology, Shanghai Jiao Tong University, Shanghai, 200240, People's Republic of China |
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Abstract: | Ag2S nanoparticles in hyperbranched polyurethane matrix were prepared through the in situ reaction with thioacetamide as the sulfur source at room temperature. Transmission electron microscopic analysis revealed a uniform spherical shape for Ag2S nanoparticles, with an average size of about 4-10 nm and a narrow size distribution. X-ray powder diffraction and UV-vis spectroscopy were also used to characterize the obtained nanoparticles |
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Keywords: | nanoparticle hyperbranched polyurethane thioacetamide. |
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