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Evolved gas analysis with skimmer interface and ion attachment mass spectrometry for burnout monitoring of organic additives in ceramic processing
Authors:Tsugoshi Takahisa  Ito Nanaka  Nagaoka Takaaki  Watari Koji
Affiliation:Advanced Sintering Technology Group, Advanced Manufacturing Research Institute, National Institute of Advanced Industrial Science and Technology (AIST), Japan
Abstract:A monitoring of the individual pyrolysis of mixed polymer as a binder for ceramic processing was carried out as an application of evolved gas analysis-mass spectrometry (EGA-MS) with a skimmer interface and ion attachment mass spectrometry (IAMS). It could detect characteristic species evolved by the pyrolysis of the organic additives, according to the instrumental advantages as the transmission of the gaseous species with no transformation by the skimmer interface and complete soft ionization for gaseous species by IAMS technique. Further, the pyrolysis behavior of blended polymers as a binder could be monitored individually as EGA curves of characteristic species evolved by the pyrolyses.
Keywords:Evolved gas analysis, EGA   Mass spectrometry   Skimmer interface   Pyrolysis   Ion attachment mass spectrometry, IAMS   Binder   Monitoring
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