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Parameter optimization in microwave-assisted distillation of frankincense essential oil
Authors:Mohammad Turk  Carole Mathe  Anne-Sylvie Fabiano-Tixier  Diego Carnaroglio  Farid Chemat
Institution:1. UMR408 ”Sécurité et qualité des produits d''origine végétale“, Université d''Avignon et des pays de Vaucluse, 84000 Avignon, France;2. UMR7263/IRD237, Avignon University/CNRS/IRD/AMU, Restoration Engineering of Natural and Cultural Heritage, 84000 Avignon, France;3. Milestone, Via Fatebenefratelli, 1-5, 24010 Bergamo, Sorisole, Italy;4. Dipartimento di Scienza e Tecnologia Del Farmaco, Centre for Nanostructured Interfaces and Surfaces, Università Degli Studi di Torino, Via Pietro Giuria 9, 10125 Torino, Italy
Abstract:The essential oil of Boswellia species is extracted by the conventional method of hydrodistillation (HD). In this study, we aimed to compare this reference to microwave-assisted distillation (MAD) at different power densities. The results showed that microwave extraction can result in a substantial reduction (48 min against 180 min for reference) of the batch time when the power density of 2 W/g is applied. Also, the energy consumed by the new process is 2.7 times less than HD. The essential oil produced by MAD has a chemical composition different from that of reference treatment. Although microwave treatment increased the proportions of the main components (α-thujene and α-pinene), the opposite tendency was observed for o-cymene, estragole, methyl eugenol, and δ-guaiene. A 26.5% decrease in oil extracted by MAD at 1 W/g is required to achieve 50% inhibition of the DPPH radical compared to HD. In conclusion, MAD is a promising technology for producing olibanum oil with new qualitative attributes.
Keywords:Frankincense  Olibanum  Distillation  Energy  Kinetics  Yield
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