On-line coupling of miniaturized solid-phase extraction and microcolumn liquid-phase separations |
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Authors: | Saito Yoshihiro Jinno Kiyokatsu |
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Affiliation: | School of Materials Science, Toyohashi University of Technology, Toyohashi 441-8580, Japan. |
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Abstract: | On-line coupling of miniaturized solid-phase extraction methods and microcolumn separation techniques are reviewed. A conventional solid-phase micro-extraction device and fiber-in-tube solid-phase extraction was employed as the sample preparation method. In the fiber-in-tube technique, a novel fibrous polymeric material was introduced as the extraction medium for the microscale sample preparation step which could be directly coupled with microcolumn liquid-phase separation systems, such as microcolumn liquid chromatography, capillary electrophoresis, and capillary electrochromatography. The applications of these hyphenated systems, consisting of the sample preparation and separation processes, are also reviewed. |
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