| 二苄基N,N-二甲基荒酸锡的合成及晶体结构研究 |
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| 引用本文： | 朱德中,张如芬,尹汉东,马春林. 二苄基N,N-二甲基荒酸锡的合成及晶体结构研究[J]. 合成化学, 2002, 10(2): 126-130 |
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| 作者姓名： | 朱德中 张如芬 尹汉东 马春林 |
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| 作者单位： | 聊城师范学院化学系,山东,聊城,252059 |
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| 摘 要： | 用二苄基二氯化锡与N,N-二甲基荒酸钠反应合成了化合物(PhCH2)2Sn[S2CN(CH3)2]2,通过X-射线确定了其晶体结构,晶胞参数为单斜晶系,空间群P21/n,a=13.926(5),b=9.832(4), c=17.080(7),β=103.541(6)°, V=2273.7(15)3, Z=4.
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| 关 键 词： | 晶体结构 合成 二苄基N N－二甲基荒酸锡 有机锡化合物 |
ASynthesis and Crystal Structure of Dibenzyltin N,N-dimethyldithiocarboxylate (PhCH2)2Sn[S2CN(CH3)2]2 |
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| Abstract. ASynthesis and Crystal Structure of Dibenzyltin N,N-dimethyldithiocarboxylate (PhCH2)2Sn[S2CN(CH3)2]2[J]. Chinese Journal of Synthetic Chemistry, 2002, 10(2): 126-130 |
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| Authors: | Abstract |
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| Abstract: | The compound (PhCH2)2Sn[S2CN(CH3)2]2 was prepared by the reaction of dibenzyltin dichloride with sodium N,N-dimethyldithiocarboxylate. Its crystal structure has been determined by X-ray crystallography. It crystallizes in the monoclinic system, space group P21/n with a=13.926(5), b=9.832(4), c=17.080(7),β=103.541(6)°, V=2273.7(15)3, and Z=4. |
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| Keywords: | dibenzyltin dichloride N N dimethyldithiocarboxylate crystal structure |
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