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Radiometric determination of sulfate
Authors:D C Bogen  G A Welford
Institution:(1) Health and Safety Laboratory, U. S. Energy Research and Development Administration, 10014 New York, N.Y., (USA)
Abstract:A radiometric procedure for the determination of sulfate based upon the precipitation of barium sulfate is described with a sensitivity of about 0.01 μg/ml. Carrier-free35SO4 is added to the sample to measure the chemical recovery. The sulfate is precipitated with an excess of barium having a known specific activity of133Ba. The amount of133Ba determined by gamma counting is directly related by stoichiometry to the amount of sulfate in the precipitate.
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