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多胺螯合纤维预富集-FAAS对水体中铅的形态分析
引用本文:杨秀政. 多胺螯合纤维预富集-FAAS对水体中铅的形态分析[J]. 分析试验室, 2007, 26(1): 102-104
作者姓名:杨秀政
作者单位:西南科技大学环境与资源学院,绵阳,621010
摘    要:用棉纤维为原料, 以对均苯四甲酸酐为交联剂, 合成新型多胺螯合纤维(CC-BA-TETA), 并用该材料为分离柱的填充相, 优化其分离条件. 采用CC-BA-TETA分离富集-火焰原子吸收光谱法测定天然水体中痕量Pb的方法, 可分离出天然水体中铅的5种形态: 总铅、颗粒态铅、离子态铅、非离子态铅和总溶态铅.

关 键 词:多胺螯合纤维    分离富集  形态分析
文章编号:1000-0720(2007)01-102-03
修稿时间:2006-03-062006-05-26

Study on speciation analysis of lead in water by FAAS with enrichment on CC-BA-TETA
YANG Xiu-zheng. Study on speciation analysis of lead in water by FAAS with enrichment on CC-BA-TETA[J]. Chinese Journal of Analysis Laboratory, 2007, 26(1): 102-104
Authors:YANG Xiu-zheng
Affiliation:Department of Environment and Resource, South West University of Science and Technology, Mianyang 621000
Abstract:In this paper,a new kind of polyamines chelated cellulose CC-BA-TETA(trithylene tetraamine chelated cellulose was cross-linked by 1,2,4,5-benzenettetracarboxylic aciddianhydride) was synthesized with cotton cellulese and used as column packing to optimize conditions of separation.A method for the speciation analysis of lead in water by FAAS with enrihment on CC-BA-TETA was developed.It can measure the contents of total lead,particulate state lead,ionic state lead, non-ionic state lead and total dissolved state lead.
Keywords:Polyamines chelated cellulose   Lead   Separation and enrichment   Speciation analysis
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