| N-芳基二茂铁丙烯酰胺的合成与表征 |
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| 引用本文： | 范瑞兰,焦威,边占喜,李保国.N-芳基二茂铁丙烯酰胺的合成与表征[J].应用化学,2003,20(10):959-0. |
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| 作者姓名： | 范瑞兰 焦威 边占喜 李保国 |
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| 作者单位： | 内蒙古大学 |
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| 基金项目： | 内蒙古自治区教育厅基金 (30 0 318)，内蒙古大学青年科学基金 (2 0 2 0 42 )资助项目 |
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| 摘 要： | 二茂铁丙烯酰氯;N-芳基二茂铁丙烯酰胺的合成与表征
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| 关 键 词： | 二茂铁丙烯酰氯 N-芳基二茂铁丙烯酰胺的合成与表征 |
| 文章编号： | 1000-0518(2003)10-0959-04 |
| 收稿时间： | 2009-06-29 |
| 修稿时间： | 2003年1月22日 |
Synthesis and Characterization of N-Aryl-Ferrocenylacryl Amides |
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| FAN Rui-Lan ,JIAO Wei,BIAN Zhan-Xi,LI Bao-Guo.Synthesis and Characterization of N-Aryl-Ferrocenylacryl Amides[J].Chinese Journal of Applied Chemistry,2003,20(10):959-0. |
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| Authors: | FAN Rui-Lan JIAO Wei BIAN Zhan-Xi LI Bao-Guo |
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| Institution: | FAN Rui-Lan *,JIAO Wei,BIAN Zhan-Xi,LI Bao-Guo |
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| Abstract: | The reaction of ferrocenylacrylate with SOCl 2 using pyridine as catalyst produced ferrocenylacryl chloride(yield 45%), which in reaction with(substituted) anilines gave thirteen N-aryl-ferrocenylacryl amides( FcCH CHCONHAr). The method is time saving and easy in seperation and purification of the products. The product compounds have been characterized by elemental analysis, IR and 1H NMR spectra. The results indicate that the kind and position of the substituents in aniline ring greatly affected the conjugation system and coplanarity of the products. |
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| Keywords: | ferrocenylacrylyl chloride N-aryl-ferrocenylacryl amide synthesis |
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