The use of sodium tetraethylborate for the derivatization and analysis of selenium containing compounds |
| |
| Authors: | Steven Clark Peter J Craig |
| |
| Institution: | (1) Department of Chemistry, De Montfort University, The Gateway, P.O. Box 143, LE1 9BH Leicester, UK |
| |
| Abstract: | Several selenium containing compounds have been derivatized to diethyl selenide using sodium tetraethylborate. The evolved diethyl selenide was detected by gas chromatography interfaced with atomic absorption or mass spectroscopic methods. Derivatization was carried out on the analyte in a sealed vial using an aqueous solution of sodium tetraethylborate (2%) added by means of a syringe. |
| |
| Keywords: | sodium tetraethylborate ethylation analysis selenium |
| 本文献已被 SpringerLink 等数据库收录！ |
