| 羧基功能化离子液体修饰Pd纳米微粒的制备及结构表征 |
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| 引用本文： | 张晟卯,李健,张春丽,吴志申,张治军.羧基功能化离子液体修饰Pd纳米微粒的制备及结构表征[J].无机化学学报,2007,23(4):729-732. |
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| 作者姓名： | 张晟卯 李健 张春丽 吴志申 张治军 |
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| 作者单位： | 1. 河南大学特种功能材料重点实验室,开封,475001;中国科学院兰州化学物理研究所,固体润滑国家重点实验室,兰州,730000
2. 河南大学特种功能材料重点实验室,开封,475001 |
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| 基金项目： | 国家自然科学基金;中国科学院兰州化学物理研究所固体润滑国家重点实验室开放课题基金;河南省自然科学基金 |
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| 摘 要： | 1-methyl-3-(ω-carboxyl)decyl imidazolium bromine (C11OOHmim]Br) ionic liquid was synthesized and C11OOHmim]Br modified Pd nanoparticles were prepared in solution. The morphology and structure of Pd nanoparticles were investigated by IR, TEM, XRD, XPS. The results indicated that the Pd nanoparticles were face-centered cubic structure and the diameter was between 10～30 nm. C11OOHmim]Br was connected to the surface of Pd nanoparticles by carboxyl and Pd nanoparticles with different sizes could be obtained by varying the amount of the modifier.
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| 关 键 词： | 羧基功能化离子液体 Pd纳米微粒 结构表征 |
| 文章编号： | 1001-4861(2007)04-0729-04 |
| 修稿时间： | 2006-11-06 |
Preparation and Structural Characterization of Carboxyl-functional Ionic Liquid Modified Pd Nanoparticles |
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| ZHANG Sheng-Mao,LI Jian,ZHANG Chun-Li,WU Zhi-Shen and ZHANG Zhi-Jun.Preparation and Structural Characterization of Carboxyl-functional Ionic Liquid Modified Pd Nanoparticles[J].Chinese Journal of Inorganic Chemistry,2007,23(4):729-732. |
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| Authors: | ZHANG Sheng-Mao LI Jian ZHANG Chun-Li WU Zhi-Shen and ZHANG Zhi-Jun |
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| Institution: | 1.Special Functional Material Laboratory, Henan University, Kaifeng, Henan 475001; 2.State Key Laboratory of Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000 |
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| Abstract: | |
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| Keywords: | carboxyl-functionalized ionic liquids Pd nanoparticles structural characterization |
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