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The spectrophotometric determination of sulphate after its extraction with methyltricaprylammonium chloride into cyclohexane
Authors:D Thorburn Burns  M Bushra
Institution:Department of Analytical Chemistry, The Queen''s University of Belfast, Belfast BT9 5AG Northern Ireland
Abstract:Improvements are described to Flynn's procedure for the extraction of sulphate with Aliquat-336 and its subsequent determination as sulphuric acid. A single-point photometric measurement with sodium 2,4-dinitrophenate is applied to the determination of sulphate (ca. 10 mg kg?1) in soils, and also in sulphur in organic compounds after oxygen flask combustion.
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