A novel synthesis of perfluoroalkyl alkyl ketones |
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| Affiliation: | 1. Quantum Computing and Phytochemistry Research Laboratory, Bannari Amman Institute of Technology, Sathyamangalam 638 401, Tamil Nadu, India;2. Department of Chemistry, Bannari Amman Institute of Technology, Sathyamangalam 638 401, Tamil Nadu, India;3. Department of Physics, Bannari Amman Institute of Technology, Sathyamangalam 638 401, Tamil Nadu, India;4. Department of Physics, Vivekanandha College of Arts and Science for Women (Autonomous), Tiruchengode 637205, India;1. Department of Materials Chemistry, Faculty of Science and Technology, Ryukoku University, Otsu, Shiga 520-2194, Japan;2. Department of Chemistry and Biochemistry, California State University Long Beach, 1250 Bellflower Blvd., Long Beach, CA 90840, USA;1. Department of Organic Chemistry, Medical University of Gdańsk, Al. Gen. J. Hallera 107, 80-416 Gdańsk, Poland;2. Department of Chemical Technology of Drugs, Medical University of Gdańsk, Al. Gen. J. Hallera 107, 80-416 Gdańsk, Poland;3. Pharmaceutical Department, Poznan University of Medical Sciences, 60-780 Poznań, Poland;4. Faculty of Chemistry, Adam Mickiewicz University, 61-614 Poznań, Poland;5. Department of Pharmaceutical Microbiology, Medical University of Gdańsk, Al. Gen. J. Hallera 107, 80-416 Gdańsk, Poland;1. National Key Laboratory of Green Pesticide, Key Laboratory of Green Pesticide and Agricultural Bioengineering, Ministry of Education, Guizhou University, Huaxi District, Guiyang 550025, China;2. School of Chemistry, Chemical Engineering, and Biotechnology, Nanyang Technological University, Singapore 637371, Singapore |
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| Abstract: | A novel synthesis of perfluoroalkyl alkyl ketones via the hydrolysis of fluorinated β-ketophosphonium salts is described. In view of the fact that a one-pot reaction without isolation of intermediates and the total yield in 2 steps reaches 37-78%, the present method provides a convenient synthesis of the title compounds. |
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