| 盐酸羟胺的间接分光光度法测定 |
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| 引用本文： | 杨明,杨丰科. 盐酸羟胺的间接分光光度法测定[J]. 分析测试学报, 1999, 18(3): 64-66 |
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| 作者姓名： | 杨明 杨丰科 |
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| 作者单位： | 1. 山西师范大学化学系,临汾,041004
2. 青岛化工学院有机化学教研室,青岛,266042 |
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| 摘 要： | 拟定了在铁（Ⅲ）—２－［２－（６－甲基苯并噻唑）偶氮］－５－二乙氨基苯甲酸（６ＭｅＢＴＡＥＢ）络合物和十二烷基硫酸钠存在下盐酸羟胺的间接分光光度测定方法，回收试验表明该法准确可靠，方便快捷。同时测定了盐酸羟胺与Ｆｅ（Ⅲ）－６＿Ｍｅ＿ＢＴＡＥＢ络合物的反应比。
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| 关 键 词： | 盐酸羟胺 分光光度法 间接法 铁(Ⅲ)-2-[2-(6-甲基苯并噻唑)偶氮]-5-二乙氨基苯甲酸络合物 |
Indirect Spectrophotometry of Hydroxylamine Hydrochloride |
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| Yang Ming,Yang Fengke. Indirect Spectrophotometry of Hydroxylamine Hydrochloride[J]. Journal of Instrumental Analysis, 1999, 18(3): 64-66 |
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| Authors: | Yang Ming Yang Fengke |
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| Abstract: | Hydroxylamine hydrochloride was determined by indirect spectrophotometric method based on the formation of Fe()-2 yl)azo] 5 diethylaminobenzoic acid(6 Me BT_AEB) complex which was the product of the redox reaction between hydroxylamine hydrochloride and Fe()-6 Me BTAEB in the presence of sodium dodecylsulfate.The reaction ratio of the two reactants was evaluated. The proposed method was applied to analysis of industrial grade of hydroxylamine hydrochloride with satisfactory results. |
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| Keywords: | Hydroxylamine hydrochloride Spectrophotometry Indirect method Fe()-2 5 diethylaminobenzoic acid |
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