Microwave-assisted synthesis of 3-substituted-6-ferrocene methylene-1,2,4-triazolo[3,4-<Emphasis Type="Italic">b</Emphasis>]-1,3,4-thiadiazoles |
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| Authors: | Yuting Liu Hong Xin Jingyi Yin Dawei Yin |
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| Institution: | 1.College of Chemistry and Chemical Engineering, Key Laboratory of Auxiliary Chemistry and Technology for Chemical Industry, Ministry of Education,Shaanxi University of Science and Technology,Xi’an,China |
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| Abstract: | A series of triazolo-thiadiazole derivatives containing ferrocene were synthesized under microwave assistance. Compared with the phosphorus oxychloride method, the microwave method has the advantages of simple operation, short reaction time, fast reaction rate and high yield. The effects of different reaction conditions were explored, and under the optimized conditions, the products were obtained in good yields (up to 80%). |
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