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A Simple One-pot Synthesis of Indeno[2,1-f]quinolin-3-one Derivatives under Microwave Irradiation
Authors:PENG Juhua  JIA Runhong  XU Yajuan  TU Shujiang  MA Ning  ZHANG Ge
Institution:1. School of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou, Jiangsu 221116, China;2. Lianyungang Teachers' College, Lianyungang, Jiangsu 222006, China;3. Tel. & Fax: 0086‐0516‐83500065
Abstract:A series of new indeno2,1‐f]quinolin‐3(2H)‐one derivatives were synthesized by a reaction of aromatic aldehyde with Meldrum's acid (2,2‐dimethyl‐1,3‐dioxane‐4,6‐dione) and 9H‐fluoren‐2‐amine under microwave irradiation without catalyst in glacial acetic acid. This reaction has notable advantages of short reaction time, high yield and convenient operation.
Keywords:microwave irradiation  indeno[2  1‐f]quinolin‐3(2H)‐one  one‐pot protocol  synthesis
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