| HPLC法测定红花罂粟中蒂巴因的含量 |
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| 引用本文： | 宋小兰,刘强. HPLC法测定红花罂粟中蒂巴因的含量[J]. 分析测试技术与仪器, 2005, 11(2): 146-148 |
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| 作者姓名： | 宋小兰 刘强 |
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| 作者单位： | 1. 甘肃省药物碱厂,甘肃,733006
2. 甘肃省农垦农业研究院,甘肃,733006 |
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| 摘 要： | 建立了一种采用辛烷基键合硅胶为填充剂的固相小柱纯化样品，用高效液相色谱对红花罂粟中蒂巴因含量进行测定的方法。对照品在0．01～0．09g／L浓度范围内线性良好，标准曲线的相关系数为0．9992；样品中蒂巴因的平均回收率为100．08％，RSD为0．48％。该测定方法简便快捷，准确度高，可以成为红花罂粟植物的质量控制方法。
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| 关 键 词： | 固相萃取 高效液相色谱法 蒂巴因 红花罂粟 |
| 文章编号： | 1006-3757(2005)02-0146-03 |
| 收稿时间： | 2005-06-01 |
| 修稿时间： | 2005-06-01 |
Determination of Thebaine in Red Poppy by High Performance Liquid Chromatography |
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| SONG Xiao-lan and LIU Qiang. Determination of Thebaine in Red Poppy by High Performance Liquid Chromatography[J]. Analysis and Testing Technology and Instruments, 2005, 11(2): 146-148 |
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| Authors: | SONG Xiao-lan and LIU Qiang |
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| Affiliation: | Medical Alkaloid Factory of Gansu Province, Wuwai 733006, China;Gansu State Farms Academy of Agricultural Research, Wuwai 733006, China |
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| Abstract: | A method of determining thebaine in red poppy with solid-phase extraction-high performance liquid chromatography was developed. There is a good linear relationship within the range of 0.01~0.09 g/L. The correlation coefficient for the thebaine was greater than 0.999 2. The average rate of recovery for the reference substance was 100.08% and the relative standard deviation was 0.48%. The results showed that the proposed method was simple, rapid and accurate. The method has been applied to the determination of the thebaine in red poppy. |
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| Keywords: | solid phase extraction HPLC thebaine red poppy. |
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