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NMR characterisation of unstable solvent and dihydride complexes generated at low temperature by in-situ UV irradiation
Authors:Godard Cyril  Callaghan Philip  Cunningham Jenny L  Duckett Simon B  Lohman Joost A B  Perutz Robin N
Affiliation:Department of Chemistry, University of York, Heslington, York, UK YO10 5DD.
Abstract:Low temperature in-situ UV irradiation of toluene solutions containing bis(alkene)rhodium complexes and parahydrogen in conjunction with NMR monitoring enables the characterisation of unstable eta 2-solvent complexes and dihydrogen activation products.
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