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Evaluation of microstructures and properties of bulk mesoporous silica
Authors:Atsushi Nakahira  Hidezumi Nagata  Takamasa Onoki  Yuki Yamasaki
Institution:(1) Osaka Prefecture University, 1-1, Gakuen-cho, Naka-ku, 599-8531 Sakai, Osaka, Japan;(2) Tokyo Institute of Technology, 4259, Nagatsuta-cho, Midori-ku, 226-8503 Yokohama, Japan;(3) Hosei University, 4342, Aihara-cho, Machida, 194-0298 Tokyo, Japan
Abstract:Synthesis of mesoporous MCM-type bulks prepared by hydrothermal hot-pressing (HHP) method using MCM-type mesoporous powder was attempted. Scanning electron microscopy (SEM), bulk density measurement, N2 adsorption-desorption isotherms and formaldehyde adsorption test have been employed to characterize the bulky products. As a result, we succeeded in preparing a dense and strong mesoporous bulks with high BET over 1000 m2/g through the hydrothermal hot-pressing method under appropriate conditions.
Keywords:Mesoporous silica  hydrothermal hot-pressing  adsorption  formaldehyde
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