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热丝法低温制备多晶硅薄膜微结构的研究
引用本文:王丽春,张贵锋,侯晓多,姜辛.热丝法低温制备多晶硅薄膜微结构的研究[J].人工晶体学报,2007,36(6):1372-1376,1398.
作者姓名:王丽春  张贵锋  侯晓多  姜辛
作者单位:大连理工大学材料科学与工程学院三束材料改性国家重点实验室,大连,116024
基金项目:教育部留学回国人员科研启动基金
摘    要:采用热丝化学气相沉积法(HFCVD)在普通玻璃衬底上低温沉积多晶硅薄膜。利用XRD、拉曼光谱和原子力显微镜(AFM)研究了灯丝与衬底间距(5~10mm),灯丝温度(1800~1400℃)和衬底温度(320~205℃)对薄膜晶体取向、晶化率、晶粒尺寸以及形貌的影响规律。结果表明,随着热丝与衬底间距增加,多晶硅薄膜的晶化率和晶粒尺寸明显减小;随热丝温度的降低,薄膜的晶化率都出现了大致相同的规律:先不断增大后突然大幅减小。

关 键 词:热丝化学气相沉积  多晶硅薄膜  择优取向  晶化率  晶体形貌
文章编号:1000-985x(2007)06-1372-05
收稿时间:2007-04-09
修稿时间:2007-07-08

Microstructure of Poly-Si Thin Films Prepared by Hot-filament Chemical Vapor Deposition at Low-temperature
WANG Li-chun,ZHANG Gui-feng,HOU Xiao-duo,JIANG Xin.Microstructure of Poly-Si Thin Films Prepared by Hot-filament Chemical Vapor Deposition at Low-temperature[J].Journal of Synthetic Crystals,2007,36(6):1372-1376,1398.
Authors:WANG Li-chun  ZHANG Gui-feng  HOU Xiao-duo  JIANG Xin
Abstract:Polycrystalline silicon thin films were prepared by hot-filament chemical vapor deposition(HFCVD) on glass at low-temperatures.The preferential growth orientation,the crystalline fraction and the grain sizes of poly-Si films significantly depend on the filament temperature and the distance of substrate to filament.The effects of deposition parameters on the microstructure of films were characterized by X-ray diffraction(XRD),Raman spectrum and atomic force microscopy(AFM).It was found that the crystalline fraction and the grain sizes of poly-Si films distinctly decreased with the increasing distance of substrate to filament.The crystalline fraction of poly-Si films continuously increased to a maximum value and then rapidly reduced with decreasing filament temperature.
Keywords:HFCVD  poly-Si thin film  preferential orientation  crystalline fraction  crystal morphology
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