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Synthesis, spectral characteristics, and some properties of methylammonium sulfamate monohydrate. A new route to sulfamic acid derivatives |
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| Authors: | R. E. Khoma A. V. Mazepa V. O. Gelmboldt A. A. Shestaka L. V. Koroeva M. D. Tsapko A. A. Ennan |
| Affiliation: | 1. Mechnikov National University, Dvoryanskaya ul. 2, Odessa, 65026, Ukraine 2. Physicochemical Institute for Human and Environmental Protection, Ministry of Education and Science and National Academy of Sciences of Ukraine, ul. Preobrazhenskaya, Odessa, 65026, Ukraine 3. Bogatskii Physicochemical Institute, National Academy of Sciences of Ukraine, Lustdorfskaya doroga 86, Odessa, 65080, Ukraine 4. Odessa State Medical University, per. Valikhovskogo 2, Odessa, 65026, Ukraine 5. Shevchenko National University, Volodymyrska vul. 64, Kiev, 01033, Ukraine |
| Abstract: | Redox transformations of the products of reactions of the CH3C(S)NH2-SO2-H2O system components yield methylammonium sulfamate monohydrate [CH3NH3]+[OSO2NH2]? · H2O and elemental sulfur. The synthesized compound was characterized by IR, 1H and 13C NMR, and mass spectroscopy and some of its properties were studied. |
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